Easy and green synthesis of TiO2 (Anatase and Rutile): Estimation of crystallite size using Scherrer equation, Williamson-Hall plot, Monshi-Scherrer Model, size-strain plot, Halder- Wagner Model

Sahadat Hossain, Md.; Ahmed, Samina

doi:10.1016/j.rinma.2023.100492

Results in Materials

2023

DOI: 10.1016/j.rinma.2023.100492

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Easy and green synthesis of TiO2 (Anatase and Rutile): Estimation of crystallite size using Scherrer equation, Williamson-Hall plot, Monshi-Scherrer Model, size-strain plot, Halder- Wagner Model

Md. Sahadat Hossain,

Samina Ahmed

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Cited by 22 publications

References 58 publications

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Synthesis and Characterization of Nano‐Crystallite Triple Super Phosphate (TSP) from Marine Mollusk Waste: Babylonia japonica, Oliva sayana, and Conasprella bermudensis

Kawsar,

Sahadat Hossain,

Akter

et al. 2024

ChemistryOpen

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The study aims to synthesize nano‐crystallite TSP using renewable, low‐cost, waste marine mollusk from three different species such as Babylonia japonica, Oliva sayana, and Conasprella bermudensis. The molar ratio of phosphate to calcium in triple superphosphate [TSP, Ca(H2PO4)2.H2O] significantly impacts its properties and fertilizer performance, in this case, we kept the ratio to 2. Raw TSP has a high phosphate content and lower calcium content. The synthesized TSP was analyzed using various techniques including TGA, XRD, EDX, FT‐IR, and SEM. The study utilized multiple XRD model equations to analyze crystallite size ( ), with all models except the Liner straight‐line method providing higher estimates for synthesized TSP. Furthermore, the values for stress (2×107 to 4×107 N/m2), strain (4×10−4 to 9×10−4), as well as energy density (4.54×103 to 16.27×103 J/m3) were also calculated for the synthesized product. However, the preferential growth calculation indicates that (010), (021), and (020) planes are the most thermodynamically stable planes for the growth of the synthesized TSP. Apart from that, FTIR result confirms that CaO, −OH, as well as PO43− functional groups are present in the synthesized products. This research suggests that marine mollusks can be utilized as a calcium precursor for P‐fertilizer and 60 % phosphoric acid, thereby reducing production costs by eliminating additional dehydrating. Additionally, waste marine mollusk shells could be utilized as an alternative to the production of phosphate‐based fertilizer.

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Synthesis and Characterization of Nano‐Crystallite Triple Super Phosphate (TSP) from Marine Mollusk Waste: Babylonia japonica, Oliva sayana, and Conasprella bermudensis

Kawsar,

Sahadat Hossain,

Akter

et al. 2024

ChemistryOpen

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Facile sol-gel synthesis of ZnAl2O4 spinel nanoceramics for photocatalytic applications: H2 production and MB dye degradation

Ávalos-Marrón,

Diaz-Torres,

Gómez-Solís

et al. 2024

J Sol-Gel Sci Technol

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Thermo-catalytic depolymerization of lignin over Pd-based catalysts: Role of catalyst support on monoaromatics selectivity

Colina,

Ortega,

Norambuena-Contreras

et al. 2025

Biomass and Bioenergy

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Easy and green synthesis of TiO2 (Anatase and Rutile): Estimation of crystallite size using Scherrer equation, Williamson-Hall plot, Monshi-Scherrer Model, size-strain plot, Halder- Wagner Model

Cited by 22 publications

References 58 publications

Synthesis and Characterization of Nano‐Crystallite Triple Super Phosphate (TSP) from Marine Mollusk Waste: Babylonia japonica, Oliva sayana, and Conasprella bermudensis

Synthesis and Characterization of Nano‐Crystallite Triple Super Phosphate (TSP) from Marine Mollusk Waste: Babylonia japonica, Oliva sayana, and Conasprella bermudensis

Facile sol-gel synthesis of ZnAl2O4 spinel nanoceramics for photocatalytic applications: H2 production and MB dye degradation

Thermo-catalytic depolymerization of lignin over Pd-based catalysts: Role of catalyst support on monoaromatics selectivity

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