This paper introduces an instructional framework for process identification, combining theoretical concepts with practical laboratory exercises, focusing particularly on the identification of first‐order‐plus‐time‐delay models. Our methodology emphasizes guiding students through the various stages involved in the system identification process, namely mastering techniques, such as data acquisition and preprocessing, identification and validation stages, and method comparison. The laboratory assignment is structured into three distinct stages: an initial prelab task working with simulated data, the hands‐on work with laboratory equipment, and the assignment report writing and oral presentation. The assessment of students' learning outcomes is conducted using a detailed rubric. Feedback from a focus group interview indicates that the majority of students appreciated the well‐balanced content, highlighting a strong link between theoretical concepts and practical application.