Effect of C/Ti ratio on self-propagating high-temperature synthesis reaction of Sn–Ti–C system for fabricating Ti2SnC ternary compounds

Synthesis of Ti2SnC under Optimized Experimental Parameters of Pressureless Spark Plasma Sintering Assisted by Al Addition

“…In consideration of the results by Li et al [15] and the present work, and combined with the gure diagram ( Figure 8) [32], the possible reaction routes are proposed as follows:…”

“…Up to now, Ti 2 SnC has been synthesized by various methods mostly using the powder mixture of Ti/Sn/C elements or their compounds [10][11][12][13][14]. In consideration of large-scale fabrication possibility, self-propagating hightemperature synthesis (SHS), and pressureless sintering have been paid much attention due to their simplicity and easy operation [15]. However, unexpected impurities, such as TiC, Ti 6 Sn 5 , and or Sn, are usually found to accompany the formation of Ti 2 SnC in these processes.…”

Effect of Milling Time on Phase Composition and Microstructure of Ti-Sn-C Powder

“…At present, the synthesis of more successful methods of pressure sintering, liquid-solid reaction method, hot isostatic pressing method [4][5][6]. Yu [7] and so on Ti / Sn / C element powder by 2 1 1 molar ratio of ingredients, at a certain temperature self-propagating reaction, high purity Ti 2 SnC powder. But the above methods are high temperature synthesis, the experimental process is relatively complex.…”