2008
DOI: 10.1016/j.apsusc.2008.04.109
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Effect of different trimethyl silylating agents on the hydrophobic and physical properties of silica aerogels

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Cited by 122 publications
(48 citation statements)
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“…The modification by MTCS contributed to the formation of a low‐energy surface of the cellulose aerogels because of the replacement of surface hydrophilic hydroxyl groups on the cellulose with plentiful hydrophobic groups; this led to the generation of hydrophobicity . Figure (a) presents the FTIR spectra of the NFC aerogels and the MTCS‐treated aerogels.…”
Section: Resultsmentioning
confidence: 99%
“…The modification by MTCS contributed to the formation of a low‐energy surface of the cellulose aerogels because of the replacement of surface hydrophilic hydroxyl groups on the cellulose with plentiful hydrophobic groups; this led to the generation of hydrophobicity . Figure (a) presents the FTIR spectra of the NFC aerogels and the MTCS‐treated aerogels.…”
Section: Resultsmentioning
confidence: 99%
“…However, there is not any report on the preparation of hydrophobic silica film by one-step sol-gel process using Isooctyltrimethoxysilane as a modifying agent. Many reports are available for the evaluation of the effect of the hydrophobic agent on the water repellency [1,24,28,[32][33][34][35]. They reported that in single-step sol-gel method with increasing the concentration of the hydrophobic agent, contact angle increased.…”
Section: Page 3 Of 34mentioning
confidence: 98%
“…The weight loss of 5% appear in the TG curves with respect to the temperature within 290e550 C for the aerogels at I ¼ 0.2 and I ¼ 0.8. Meanwhile, the sharp exothermic peak at around 300 C and 450 C in the DTA curves attributed to the condensation among SieOH and oxidation of SieCH 3 to SieOH [27,28]. Therefore, the transition temperature from hydrophobic to hydrophilic was assessed as around 450 C, which corresponds to the disappearance temperature of the SieCH 3 groups developed by the surface chemical modification by MTES.…”
Section: Tg-dta Studies and Thermal Stabilitymentioning
confidence: 99%