Effect of High-Energy Ball Milling Time on the Density and Mechanical Properties of W-7%Ni-3%Fe Alloy

Нохрин, А. В.; Малехонова, Н. В.; Чувильдеев, В. Н.; Мелехин, Н. В.; Bragov, A. M.; Filippov, A. G.; Болдин, М. С.; Lantsev, E. A.; Сахаров, Н. В.

doi:10.3390/met13081432

Cited by 6 publications

(1 citation statement)

References 83 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…MA is a powder technology that is based on welding, fracturing, and rewelding powder particles during the high-energy ball milling process [55][56][57][58][59]. The severe plastic deformation accumulated during MA provides the nano-grained structure with high dislocation density and vacancy concentration [60]. Large concentrations of the lattice defects are conductive to high diffusivity, which increases the solubility of the alloying elements.…”

Section: Introductionmentioning

confidence: 99%

The Microstructure and Properties of Al–Mn–Cu–Zr Alloy after High-Energy Ball Milling and Hot-Press Sintering

Yakovtseva,

Mochugovskiy,

Prosviryakov

et al. 2024

Metals

View full text Add to dashboard Cite

In the present research an Al–7.7%Mn–4.9%Zr–3.2%Cu (wt%) alloy was processed by mechanical alloying (MA) followed by hot press sintering. The microstructure, phase composition, and mechanical properties of the MA granules and sintered samples were investigated. The dissolution of Mn, Zr, and Cu with further precipitation of the Al6Mn phase were observed during high-energy ball milling. In the alloy processed without stearic acid after milling for ~10 h, an Al-based solid solution with ~4.9 wt%Zr, ~3.2 wt%Cu and a ~5 wt%Mn with a grain size of ~16 nm and a microhardness of ~530 HV were observed. The addition of stearic acid facilitated Mn dissolution and precipitation of the Al6Mn phase during milling but led to the formation of the ZrH2 phase that decreased the Zr solute and the microhardness. Precipitation of the Al6Mn, L12–Al3Zr, and Al2Cu phases during annealing and sintering of the MA granules in the temperate range of 350–375 °C was observed, and an additional Al20Cu2Mn3 phase was precipitated at 400–450 °C. Hot-press sintering at 450 °C provided a low fraction of cavities of ~1.5%, the yield strength of 1100 MPa, ultimate compressive strength of 1200 MPa, strain at fracture of 0.5% at room temperature, the yield strength of 380 MPa, ultimate compressive strength of 440 MPa, and strain at fracture of 3.5% at 350 °C. The microstructural evolution during high-temperature deformation on the sample surface was studied and the differences in deformation behavior for the alloys sintered at different temperatures were discussed.

show abstract