Effect of Hydrochloric Acid on Formation of Nanocrystalline Bismuth Phosphate Synthesized via Hot Injection Method

Lee, Siew Ling; Yong, Shih Ween; Hartini, K. O.

doi:10.14233/ajchem.2013.14507

Asian J. Chem.

2013

DOI: 10.14233/ajchem.2013.14507

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Effect of Hydrochloric Acid on Formation of Nanocrystalline Bismuth Phosphate Synthesized via Hot Injection Method

Siew Ling Lee¹,

Shih Ween Yong²,

K. O. Hartini³

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Solvothermal synthesis and characterization of hierarchical spindle-like BiPO₄aggregates

et al. 2016

MATEC Web of Conferences

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Abstract. Monodispersed spindle-like BiPO 4 aggregates with uniform morphology and size were prepared by a solvothermal route with ethylene glycol (EG)/water as mixed solvent, bismuth nitrate and sodium tripolyphosphate (STPP) as raw materials. The products were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and UV-vis absorption spectroscopy. The results indicate that obtained BiPO4 products are hexagonal phase and have good crystallinity and high purity. Additionally, it is found that the both STPP and mixed solvent play a crucial role in the formation of the spindle-like BiPO 4 aggregates, which are constructed through oriented aggregation of nanoparticles. The possible formation process was initially presented. Moreover, the bandgap energy of these novel spindle-like BiPO 4 aggregates is also estimated as 3.46eV from the UV-vis absorption spectrum.

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Solvothermal synthesis and characterization of hierarchical spindle-like BiPO₄aggregates

et al. 2016

MATEC Web of Conferences

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Effect of Hydrochloric Acid on Formation of Nanocrystalline Bismuth Phosphate Synthesized via Hot Injection Method

Cited by 1 publication

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Solvothermal synthesis and characterization of hierarchical spindle-like BiPO₄aggregates

Solvothermal synthesis and characterization of hierarchical spindle-like BiPO₄aggregates

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Effect of Hydrochloric Acid on Formation of Nanocrystalline Bismuth Phosphate Synthesized via Hot Injection Method

Cited by 1 publication

References 0 publications

Solvothermal synthesis and characterization of hierarchical spindle-like BiPO4aggregates

Solvothermal synthesis and characterization of hierarchical spindle-like BiPO4aggregates

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Solvothermal synthesis and characterization of hierarchical spindle-like BiPO₄aggregates

Solvothermal synthesis and characterization of hierarchical spindle-like BiPO₄aggregates