Effect of microwave method on jasminaldehyde synthesis using solvent-free over Mg–Al–NO3 hydrotalcite catalyst

Houssaini, Jamal; Naciri Bennani, Mohammed; Arhzaf, Said; Ziyat, Hamid; Alaqarbeh, Marwa

doi:10.1016/j.arabjc.2023.105316

Arabian Journal of Chemistry

2023

DOI: 10.1016/j.arabjc.2023.105316

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Effect of microwave method on jasminaldehyde synthesis using solvent-free over Mg–Al–NO3 hydrotalcite catalyst

Jamal Houssaini,

Mohammed Naciri Bennani,

Said Arhzaf

et al.

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2024

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Revisiting hydrotalcite synthesis: Efficient combined mechanochemical/coprecipitation synthesis to design advanced tunable basic catalysts

Nope,

Sathicq,

Martínez

et al. 2024

Nanotechnology Reviews

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Hydrotalcite materials (HTs) were synthesized by a facile and swift combined mechanochemistry/coprecipitation approach, and their catalytic activity was evaluated and compared with conventionally synthesized hydrotalcites (co-precipitation method) in the Knoevenagel condensation between furfural and ethyl cyanoacetate/malononitrile. Characterization and catalytic activity results clearly demonstrate that the proposed combined mechanochemical/coprecipitation approach provides an improvement in crystallinity, morphology, tunable basicity, and textural properties (higher surface area and enhanced surface properties) as compared to HTs obtained via conventional coprecipitation methods. In addition, mechanochemically synthesized HTs largely improve catalytic activities, including conversion and product selectivity to Knoevenagel condensation products under solventless conditions, short reaction times, or reaction at room temperature as compared to conventional counterparts (e.g., 30–40 vs > 99% product yields).

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Revisiting hydrotalcite synthesis: Efficient combined mechanochemical/coprecipitation synthesis to design advanced tunable basic catalysts

Nope,

Sathicq,

Martínez

et al. 2024

Nanotechnology Reviews

View full text Add to dashboard Cite

show abstract

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Effect of microwave method on jasminaldehyde synthesis using solvent-free over Mg–Al–NO3 hydrotalcite catalyst

Cited by 1 publication

References 30 publications

Revisiting hydrotalcite synthesis: Efficient combined mechanochemical/coprecipitation synthesis to design advanced tunable basic catalysts

Revisiting hydrotalcite synthesis: Efficient combined mechanochemical/coprecipitation synthesis to design advanced tunable basic catalysts

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