ABSTRACT:Oil palm empty fruit bunch (EFB), a natural polymeric material from the palm oil tree, is a potential precursor for making carbon for advanced materials applications because of its continuous generation in large quantities as a low cost by-product of the palm oil mill; annual production of EFB in Malaysia is approximately 2 million tonnes. Powders of natural pyropolymer having self-adhesion property, NPP1, NPP2, and NPP3, were prepared by precarbonizing the EFB, EFB treated with acid (1% HCL), and alkaline (1% NaOH) respectively. Green bodies of carbon pellets prepared from the NPP1, NPP2, and NPP3 were carbonized up to 1000• C using a multistep heating profile. Hardness of the Correspondence to: M. Deraman;