Effect of Short Attritor-Milling of Magnesium Alloy Powder Prior to Spark Plasma Sintering

Abstract

The spark plasma sintering (SPS) technique was employed to prepare compacts from (i) gas-atomized and (ii) attritor-milled AE42 magnesium powder. Short attritor-milling was used mainly to disrupt the MgO shell covering the powder particles and, in turn, to enhance consolidation during sintering. Compacts prepared by SPS from the milled powder featured finer microstructures than compacts consolidated from gas-atomized powder (i.e., without milling), regardless of the sintering temperatures in the range of 400–550 °C. Furthermore, the grain growth associated with the increase in the sintering temperature in these samples was less pronounced than in the samples prepared from gas-atomized particles. Consequently, the mechanical properties were significantly enhanced in the material made of milled powder. Apart from grain refinement, the improvements in mechanical performance were attributed to the synergic effect of the irregular shape of the milled particles and better consolidation due to effectively disrupted MgO shells, thus suppressing the crack formation and propagation during loading. These results suggest that relatively short milling of magnesium alloy powder can be effectively used to achieve superior mechanical properties during consolidation by SPS even at relatively low temperatures.

Microstructure, Mechanical, Corrosion, and Ignition Properties of WE43 Alloy Prepared by Different Processes

“…There was residual trapped air between powder particles which allowed the surface oxidation of individual particles. The formation of oxide shell consumed Y in the near surroundings of the surface as has been already suggested in the literature [32,33,[36][37][38][39]. The original dendritic microstructure in atomized powder turned into a homogenous microstructure with fine precipitates similar to the T4Ex state.…”