Effect of short carbon fiber content on the mechanical properties of TiB₂‐based composites prepared by spark plasma sintering

Abstract

In this study, TiB2‐30 vol% SiC composites containing 0, 5, 10, and 15 vol% short carbon fibers (Cf) were produced by spark plasma sintering (SPS). The effect of carbon fiber content on microstructure, density, and mechanical properties (micro‐hardness and flexural strength) of the fabricated composites was studied. Scanning electron microscopy (SEM) results indicated that the fibers were uniformly dispersed in the TiB2–SiC matrix using wet ball milling before SPS process. Fully dense TiB2–SiC–Cf composites were achieved by SPS process at 1900°C for 10 min under 30 MPa. With the addition of fibers, the relative density of the composites did not change considerably. Mechanical tests revealed that microhardness was reduced about 19% by the incorporation of carbon fibers, whereas the flexural strength improved significantly. However, the flexural strength diminished by adding carbon fibers above to critical value (5 vol%) due to residual thermal stresses, nonhomogeneous structure and graphitization of carbon fibers. It was found that the composite with 5 vol% Cf had the highest flexural strength (482 MPa), which was enhanced by 20% compared with the TiB2–SiC composite.

Design and optimization of TiB2‐based ceramic tool materials based on fuzzy theory

“…Additionally, the incorporation of silicon carbide whiskers had led to a reinforcement effect, consequently augmenting the fracture toughness of the ceramics. Ghafuri 12 studied the effect of carbon fiber on the mechanical properties of TiB 2 ‐based ceramic tool materials by phase‐increasing method. Through an extensive array of experiments, TiB 2 30 vol.%–SiC 5 vol.% C composite ceramic tool materials with improved bending strength were optimized using high‐strength carbon fibers.…”