Aluminium 2024 based Boron fibre and Graphite-based particle reinforced Metal matrix composite (MMC) has been produced by Powder metallurgy (P/M) technique. Four different MMC with composition Al 2024 with 4% and 8% wt.% Boron fiber and 1% of Graphite has been prepared. Die has been designed and fabricated with D3 die steel. ANSYS analysis is carried out to ensure safe working of the die. Optical microscope and SEM analysis was carried out to ensure the uniform distribution of particles. XRD analysis is carried to ensure the composition of the reinforcement particles. The compacting of powders has been done at 550 MPa and sintered in electric muffle furnace at 500°C for 90 minutes. Microstructure and SEM analysis is carried out to investigate the distribution of reinforcement on matrix. It has been found that the reinforcement is distributed uniformly in the matrix. Effects of content (wt. %) on the physical and mechanical properties of composites were determined by measuring the density, hardness and Compression strength values. Both theoretical and actual density has been calculated for MMCs. Also, Porosity has determined and it has been found that as the reinforcement addition increases porosity also increases Microhardness carried out for the MMCs. It has been found that addition of Boron fibre as reinforcement Microhardness increased. Compression test was also carried out and it has been concluded the addition of boron fibre has an effect on the compressive strength but addition Graphite does not contribute much to the compressive strength. The MMCs with 8% wt. Boron fibres has highest compressive strength among the prepared MMCs