Effect of Synthetic Technology on the Properties of Co₂O₃ Powder

Abstract

Ultrafine Co2O3powder was prepared via hydrothermal synthesis. The effect of technology on the performance of the superfine Co2O3powders was investigated, and the hydrothermal parameters in preparing Co2O3were gradually improved. In addition, the morphology and grain size of the Co2O3powder were analyzed by FESEM. Results show that reducing the salt–alkali molar ratio resulted in more uniform Co2O3powder and smaller particles, with average particle size of approximately 40 nm. Reaction time displayed little effect on the Co2O3powder, but the particle size decreased with the reaction time. The concentration of salt solution remarkably affected the morphology of the Co2O3powder. Lower concentration resulted in smaller particle aggregation and particle size.