2023
DOI: 10.20944/preprints202302.0036.v1
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Effect of the Solvent on the Crystallographic and Magnetic Properties of rhenium(IV) Complexes Based on 2,2′-Bipyrimidine Ligand

Abstract: Two solvated rhenium(IV) complexes with formula [ReCl4(bpym)]·MeCN (1) and [ReCl4(bpym)]·CH3COOH·H2O (2) [bpym = 2,2'-bipyrimidine] have been prepared and characterized by means of Fourier transform infrared spectroscopy (FT–IR), scanning electron microscopy and energy dispersive X-ray analysis (SEM–EDX), single-crystal X-ray diffraction (XRD) and SQUID magnetometer. 1 and 2 crystallize in the monoclinic system with space groups P21/n and P21/c, respectively… Show more

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