Effect of Ti and Si Additions on Microstructure, Fracture Toughness and Oxidation Resistance of Nb-Mo5SiB2 Composite

Abstract

Nb-Mo 5 SiB 2 (T2)-based composites with Ti and Si additions were prepared by mechanical alloying followed by hot pressing. The phase analysis revealed that element additions induced the phase composition change. In the Ti-added Nb-T2 composite, Ti was distributed in the grain boundary as sub-micron Tirich oxide particles due to insufficient oxidation. The addition of Si turned the Nb-T2 into a complete intermetallic composite by forming Nb-silicide. The mechanical properties showed that Ti-and Si-co-added Nb-T2 composite had the highest hardness (1939 HV) and compressive strength (3445 MPa), while the Ti-added Nb-T2 composite exhibited the best toughening effect, and the fracture toughness reached 13.37 MPa m 1/2 , which were about 31% and 300% higher than that of Nb-T2 and pure polycrystalline T2, respectively. Although the Nb and Ti had excellent toughening effect on the T2 phase, it worsened the oxidation resistance of the composites.

Study on High-Temperature Oxidation Behavior of Platinum-Clad Nickel Composite Wire

“…Scientists have produced a significant amount of research on high-temperature protection coatings of nickel and nickel alloys, including the selection of coating materials [7,8], coating preparation [9,10], coating modifications [11,12], properties [13,14], and oxidationresistance mechanisms [15,16]. These research results have promoted the development of high-temperature protection fields and also provided guidance for the development of this project.…”