Reverse micro-EDM is the most suitable method for fabricating circular cross-section array microelectrodes. This work presents an experimental investigation into the effect of process parameters such as capacitance, voltage, and feed on the geometrical characteristics (diameter, length, and taper) of tungsten carbide (WC) array microelectrodes. Using a ø2 mm x 35 mm length rod of tungsten carbide, a 3x3 array of microelectrodes was fabricated with a 230 µm diameter hole in a copper sheet, providing a depth of 1.5 mm. Increasing the process parameters from 10nF capacitance, 90V voltage, and 0.3 mm/min feed to 100nF capacitance, 130V voltage, and 0.9 mm/min feed decreased the diameter by 6.75% and increased the taper of the electrodes by 3%. The ANOVA analysis indicates that capacitance, voltage, and feed significantly affect the geometrical characteristics of array microelectrodes. Using the multi-objective optimization technique grey relational analysis (GRA), it was found that at a capacitance of 10nF, a voltage of 130V, and a feed rate of 0.3 mm/min achieved the minimum deviation in the geometrical characteristics of WC array microelectrodes. This paper will help determine the hole size required to achieve the specific dimensions on the array microelectrodes and select optimal process parameters.