2013
DOI: 10.1007/s10008-013-2212-2
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Effect of water and fluoride content on morphology and barrier layer properties of TiO2 nanotubes grown in ethylene glycol-based electrolytes

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Cited by 41 publications
(32 citation statements)
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“…For Ti 4þ , the peaks are located at 458.1 eV (Ti 2p 3/2 ) and 463.8eV (Ti 2p 1/2 ). For Ti 3þ , Ti 2p 3/2 is located at 456.8 eV and Ti 2p 1/2 at 462.5 eV and for Ti 2þ , Ti 2p 3/2 and Ti 2p 1/ 2 are located at 456.1 eV and 461.4 eV respectively [24]. These contributions were also determined for the TiO 2 for comparative purposes.…”
Section: Xps Analysis Of the Filmsmentioning
confidence: 99%
“…For Ti 4þ , the peaks are located at 458.1 eV (Ti 2p 3/2 ) and 463.8eV (Ti 2p 1/2 ). For Ti 3þ , Ti 2p 3/2 is located at 456.8 eV and Ti 2p 1/2 at 462.5 eV and for Ti 2þ , Ti 2p 3/2 and Ti 2p 1/ 2 are located at 456.1 eV and 461.4 eV respectively [24]. These contributions were also determined for the TiO 2 for comparative purposes.…”
Section: Xps Analysis Of the Filmsmentioning
confidence: 99%
“…The information of chemical bonding and valence changes in reactants and products was obtained by XPS results. For the Ti 2p peak (Figure c), the binding energies of 458.6 and 464.3 eV correspond to Ti (IV) in the reactant Ti 3 O 5 and its product. The binding energies of 456.8 and 462.6 eV are due to the existence of Ti(III) in reactant Ti 3 O 5 and the binding energies of 455.8 and 461.5 eV in products originate from conductive TiO .…”
Section: Resultsmentioning
confidence: 99%
“…For the Ti 2p peak (Figure c), the binding energies of 458.6 and 464.3 eV correspond to Ti (IV) in the reactant Ti 3 O 5 and its product. The binding energies of 456.8 and 462.6 eV are due to the existence of Ti(III) in reactant Ti 3 O 5 and the binding energies of 455.8 and 461.5 eV in products originate from conductive TiO . From the XPS results, the disproportionation reaction of trivalent Ti(III) to divalent Ti(II) and tetravalent Ti(IV) in solid state is thus confirmed.…”
Section: Resultsmentioning
confidence: 99%
“…The foregoing was done because carbon is neither the main component nor it forms continuous and homogeneous layers over the electrode surfaces. 19,20 Pd3d doublet spectra were fitted using a Gaussian-Lorentzian mix function and Shirley background sub traction.…”
Section: Resultsmentioning
confidence: 99%