In this research, we will prepare spinel ferrite (Zinc ferrite) by (Sol-Gel) a method, then we will depose it with Trivalent elements Aluminum, with a ratio of (x = 0, 0.5, 0.7, 1.0) to be with following formulas Al1-xZnxFe2O4. After preparation of the samples we will study the structural properties of the compounds using X-ray diffraction (XRD), energy dispersive X-ray (EDX), and field emission scanning electron microscopy (FE-SEM), as well as using Fourier-transform infrared spectroscopy (F.T.I.R) to locate the atom in the crystal structure to find the type of ferrite. Then we will use Magnetic hysterics will be measured using A vibrating-sample magnetometer (V.S.M.) to estimate the hysterics loop of magnetism. XRD studies confirm that all the samples show a single-phase cubic spinel structure. The crystallite size of Al1-xZnxFe2O4 calculated using the Debye-Scherrer formula was found in the range of (32-38). The value of the lattice parameter 'a' is found to decrease with increasing Al 3+ content. EDX patterns confirm the compositional formation of the synthesized samples. FE-SEM micrographs show that all the samples have nano-crystalline behaviour and particles show spherical shape. The shapes show the magnetic behaviour of the prepared compound and other magnetic factors.