The effects on the estimated chemical composition of grass and silage of various methods of preparing samples for analysis were studied. The methods used for grass were: (1) oven drying and grinding, (2) freeze drying and grinding, (3) coring, (4) mincing, and (5) freezing and sawing; and for silages: (1) freezing and sawing, (2) mincing, (3) slicing with a bacon ,,~icer once or twice, and (4) chopping with a hand guillotine. Oven drying of grasses gave lowest values for dry matter (DM), soluble carbohydrate, and total N, but method of preparation had no effect on ash % or fibre %. DM and fibre contents of silages were highest in minced and frozen-sawn samples, but method of preparation had no significant effect on values for VFA, lactic acid, and ammonia.