“…Two rectangular steel plates 3 cm apart, were used as electrodes. deposited on the electrode in the form of nanopowder [32]. XRD measurements were performed on Siemens D5000 diffractometer with Ni filtered Cu-K α1,2 radiation in Bragg-Brentano geometry in the range of angles 10 0 <2θ<90 0 using a step width 0.02 0 and acquisition time 2 s/step.…”
Section: Methodsmentioning
confidence: 99%
“…Electrochemical (EC) synthesis of magnetite NPs [29][30][31][32] enables control of the final product characteristics via adjustment of the parameters in the electrolytic cell.…”
Structural and electronic properties, oxidation and aging effect of electrochemically (EC) synthesized magnetite nanopowders (NPs) are studied by means of X-ray diffraction (XRD), X-ray absorption fine structure (XAFS) and X-ray magnetic circular
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