Using waste biomass is considered one of the ways to reduce climate change. Arboreal waste biomass from pine, eucalyptus, and particularly invasive plants (Acacias) would make it possible to transform this natural resource, but needs to be adjusted to current and innovative technologies. The production of high fixed carbon biochar with this biomass would improve not only environmental aspects, but also the use of currently not susceptible materials for other types of exploitation. The objective of this study is to develop biochar from three different waste biomass materials and compare their parameters with those of the original biomass. Thermochemical conversion processes were used in a simple double chamber reactor developed for this study. Temperatures between 400 and 500 °C during 280 min were achieved and allowed to transform the initial biomass in a biochar with a high content of fixed carbon. By comparing the original biomass with the final biochar through tests of humidity, density, calorific values, fixed carbon, and cationic and elemental analysis, an increase in the parameters was confirmed. Fixed carbon of 70%, 77%, and 71% with pine, acacia, and eucalyptus biomass have been obtained, respectively, with yields between 30% and 40%. The results are favorable, particularly with acacia invasive plants, and could help in their difficult silviculture management.