In conclusion, the analysis and measurement of thermal properties are crucial for a wide range of applications in science, technology, and industry. For energy efficiency optimisation, the design of sophisticated materials, and the creation of cutting-edge technologies, it is essential to comprehend how heat is transmitted and handled within materials. Researchers can precisely evaluate thermal conductivity, heat capacity, and other thermal parameters using a variety of experimental methodologies, including both conventional and cutting-edge technologies. This enables accurate material characterisation and performance evaluation. The landscape of thermal management and energy conversion has been significantly shaped by nanostructured materials. Their distinct nanoscale characteristics provide chances to modify thermal behaviour, boost effectiveness, and add new features. Researchers are able to manage heat conduction, phonon behaviour, and charge transport through the use of designed nanostructures, which has led to breakthroughs in a variety of industries, including electronics, energy storage, thermoelectric devices, and more. In addition to promoting energy efficiency and waste heat recovery, these developments pave the path for sustainable solutions to the world’s rising energy needs and environmental problems. We are on the verge of ground-breaking discoveries that have the potential to restructure industries, enhance energy sustainability, and pave the way for a more effective and linked society as we continue to investigate and harness the complex behaviour of heat within materials.