2003
DOI: 10.1080/00304940309355845
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Efficient Synthesis of 4-Isocyano-2,2,6,6-Tetramethylpiperidine-1-Oxyl

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Cited by 18 publications
(14 citation statements)
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“…The alternative preparation of 5g and 5h from 4-isocyano-2,2,6,6-tetramethylpiperidine-1-oxyl [24] was recently reported [17].…”
Section: Resultsmentioning
confidence: 98%
“…The alternative preparation of 5g and 5h from 4-isocyano-2,2,6,6-tetramethylpiperidine-1-oxyl [24] was recently reported [17].…”
Section: Resultsmentioning
confidence: 98%
“…The reagent is able to selenate amides and formamides by substitution of the oxygen atom [40,41]. The condensation of dichlorphenylphosphine (7) with magnesium in THF [42][43][44][45][46] yields pentaphenylpentaphospholane [(PhP) 5 , (8)] SCHEME 1 (i) HCOOEt [38] (ii) COCl 2 [38] or ClCOOCCl 3 (diphosgene) (iii) Se, CHCl 3 [39] (iv) (5a-h) HX, benzene (6a,b) HX/NaX. (62% yield).…”
Section: Resultsmentioning
confidence: 99%
“…The dehydration of 2 with gaseous phosgene [38] or diphosgene leads to 4-isocyano-2,2,6,6-tetramethylpiperidine-1-oxyl (3), which was selenated with metallic selenium to give 4-isoselenocyanato-2,2,6,6-tetramethylpiperidine-1-oxyl (4) [39].…”
Section: Resultsmentioning
confidence: 99%
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