IntroductionThe remission of toxic contaminants and the use of clean energy, such as the energy of the sun, for this purpose have become popular topics for many research teams. The development of any nation in the world demands a better and major use of energy that must be efficient and have a low environmental impact. Wastewater treatment via an advanced oxidation process, which uses toxic elements from organic sources, is one of the aims of photocatalysis. The process has a high efficiency for neutralizing these toxic compounds and presents the opportunity to produce electrodes that are compatible with the environment [1]. The capability of the electrodes, chemistry process, associated cost effects and the product lifetime are related to the type of material used, and to its structure, stability, and porosity, the substrate material and shape, and the successful adhesion of the coating. These factors must be improved to reach a massive industrial application of this process. Many other factors can affect the stability of the electrode, such as substrate preparation (in particular with metallic support), the inclusion of a dopant, the solvent involved in the synthesis of the electrodes, the preparation methods and the parameters of thermal decomposition (temperature, heating rate and time) [2].Titanium oxide is one of the most studied materials for photocatalysis applications because it exhibits highly photocatalytic properties and is stable, non-toxic and relatively cheap to produce. The most efficient form of use is via the commercial nanopowders called Degussa P-25 TiO 2 [3]. However, the use of these nanopowders generates secondary costs, associate with the need for a high cost filter system to separate the particles from the treated water. To avoid this problem, studies have been conducted to obtain a material supported by a substrate that can be reused, but it must also withstand the reactor conditions during treatment. Simultaneously, these studies have tried to improve the photocatalytic activity of the material by improving the anatase phase stability, porosity distribution, superficial contact area and other variables [4,5,6,7,8]. Numerous substrates have been studied and used to fabricated these types of electrodes, including stainless steel, paper, conductive glass, titanium, ceramic foam, TiO 2 nanoneedle/nanoribbon