2024
DOI: 10.1021/acs.oprd.4c00302
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Electrochemical Cyclopropanation of 1,3-Dialkyl Bromides

Sylvain Charvet,
Clément Jacob,
Aurore Dietsch
et al.

Abstract: An electrochemical synthesis of mono-and 1,1-disubstituted cyclopropanes is demonstrated. Starting from readily available 1,3-dialkyl bromides, this method hinges on the integration of a sacrificial reductant alongside cost-effective cathode and anode materials. The refined approach eliminates the necessity for a divided cell and the use of hazardous or costly electrodes, thereby streamlining the transition of this protocol to a continuous flow system. In addition, an alternative protocol that utilizes a simpl… Show more

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