2024
DOI: 10.1002/adsc.202401349
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Electrochemically Driven Site‐Selective C(sp2)−H Bond Hydroxylation of N‐Substituted Anilines

Anil Balajirao Dapkekar,
Suman Kumar Nag,
Gedu Satyanarayana

Abstract: Organic synthesis has long been fascinated by phenolic compounds, especially their exploration of selectively hydroxylating arenes utilizing H2O as a hydroxyl source. However, phenols' low redox potential and strong reactivity frequently result in unwanted overoxidation byproducts. Here, we present an electrochemical strategy to overcome this difficulty by using electricity as an oxidant and facilitating the para‐selective hydroxylation of N‐protected anilines. This process exhibits excellent regio‐selectivity… Show more

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