“…A researcher group, led by Gupta et al [26] demonstrated that the SEM technique can be used to characterize the grain nucleation and size as a function of the processing parameters, and discovered that the key processing parameters were electrolyte concentration, current, voltage, and deposition time. Several researchers [30,42,43] have demonstrated that electrodeposited films have a nodular grain nucleation and growth, until a smooth surface is achieved. Figure 4 shows different stages of this process where it can be seen that at 0.5 h, the grain morphology corresponds to nodular grain nucleation and growth, as reported by other authors [30,42,43].…”