Electrolytic Separation of Rhodium from Iridium at Controlled Cathode Potential

MacNevin, W. M.; Tuthill, S. M.

doi:10.1021/ac60033a010

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Mercury Cathode1

Electrodeposition1

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1950

1969

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Article7

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Cited by 11 publications

(4 citation statements)

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“…Separations are also impaired by the presence of unwanted impurities in the material separated. A not unfamiliar type of contamination was reported last year by Mac-Nevin and Tuthill (13) in the separation of rhodium from iridium by controlled cathode potential techniques. After separation it was necessary to reduce the rhodium deposit in hydrogen to remove oxygen from the cathode deposit.…”

Section: Mercury Cathodementioning

confidence: 80%

Electrolytic Separations. Separation by Electroanalysis

Ashley¹

1950

Anal. Chem.

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Section: Mercury Cathodementioning

confidence: 80%

Electrolytic Separations. Separation by Electroanalysis

Ashley¹

1950

Anal. Chem.

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“…Rhodium may be separated from iridium by controlled potential electrodeposition under conditions described by MacNevin and Tuthill (83,84), but the deposit of rhodium is contaminated with oxide and cannot be quantitatively determined without first reducing it in hydrogen. Brouns (11) has studied the separation of cadmium and zinc with controlled potentials.…”

Section: Electrodepositionmentioning

confidence: 99%

Electroanalysis

Ashley¹

1952

Anal. Chem.

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“…O., Mikrochemie, 15, 12 (1934). (7) Hall. R. T., and Shaefer, W. E., "Determination of Esters," in Mitchell, J., Kolthoff, I. M., Proskauer, E. S., and Weissberger, A..…”

mentioning

confidence: 99%

“…MaeXcvin and Tuthill (7) separated the two metals by electrol-ysis using a controlled cathode potential. The method requires extensive instrumentation.…”

mentioning

confidence: 99%