Particulate matter is the term given to the tiny particles of solid or semi-solid material found in the atmosphere as suspended mixtures. The chemical complexity of airborne particles makes it imperative to consider the composition and sources of selected primary and secondary particulates deemed to be of health concern. Primary particulates are introduced into the atmosphere from a variety of natural and anthropogenic sources. Secondary particulates tend to form in the atmosphere as a result of chemical processes. 1,2 Urban particulate pollution has been recognised as a major problem in emerging mega-cities in Nigeria such as Lagos, Kano, Abuja, Aba and Port-Harcourt as a result of their rising Background. Over the past 30 years, various studies in Nigeria have monitored atmospheric particulate matter loads and elemental composition of ambient air around diverse receptor sites. Objectives. A comparative discussion of the different sampling techniques, pre-treatment and analytical methods employed between 1985 and 2015. Methods. Air pollution indices from studies covered in this review were compared to relevant guideline standards such as the World Health Organization (WHO) 24-hr guideline and the United States Environmental Protection Agency (USEPA)'s National Ambient Air Quality Standard (NAAQS) daily permissible limits for fine particles of less than 2.5 micrometers in diameter (PM 2.5) and coarse dust particles with a diameter of 10 micrometers (PM 10) in ambient air. In addition, the sources of data for the average concentrations for PM 2.5 , PM 10 and related metallic elements during 1985-2015 were assessed. Attempts were also made to compare varied particulate matter loads of atmospheric micro-environments in Nigeria with comparable microenvironments in selected cities around the world. Discussion. Results showed that PM 2.5 concentration ranged from 5-248 µg/m 3 , while PM 10 concentration ranged from 18-926 µg/m 3 , revealing that about 50% of the particulate matter loads in Nigeria exceeded both the WHO (25 µg /m 3 , 50 µg/m 3) and NAAQS (35 µg/m 3 , 150 µg/m 3) guideline limits for PM 2.5 and PM 10 respectively. PM 2.5 /PM 10 ratios for the selected studies fall below the WHO guideline (0.5-0.8), suggesting that Nigerian aerosols are mainly made up of coarse, rather than fine particles. In addition, the order of the average highest concentrations of metallic elements for PM 2.5 were magnesium (Mg) > strontium (Sr) > potassium (K) > zinc (Zn) > iron (Fe) > sodium (Na) > aluminium (Al) > chlorine (Cl) > lead (Pb) > silicon (Si), while those of PM 10 were Sr > Zn > Fe > Mg > calcium (Ca) >Na > Pb > manganese (Mn) > K > Al. Conclusions. Seasonal variation of particulate matter loads revealed higher concentrations during the dry season than during the rainy season. In addition, particulate matter loads in rural areas were generally lower than in urban areas. Wind-blown dust from the Sahara Desert is the major contributor to particulate matter loads in northern zones of the country, while sea spray and crust...