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Structural Relaxation and Crystallization of a Zr<SUB>44</SUB>Ti<SUB>11</SUB>Cu<SUB>9.8</SUB>Ni<SUB>10.2</SUB>Be<SUB>25</SUB> Bulk Metallic Glass

“…[31][32][33][34][35][36][37] Furthermore, the EXAFS technique and dilatometer measurements are believed to be useful tools for examining the change of the atomistic-scale structure. 30,[38][39][40][41] Even though the experimental information from the latter gives only the correlation between intrinsic materials properties and the atomistic-scale structural change, the former shows its ability to investigate a short-range order with a very small measurement range less than nm.…”

Effect of CaO Addition on the Properties of PbTiO3Glass Ceramic

“…Few lines of very low intensity are also observed in XRD patterns of the glass ceramic samples (X = 5, 10 and 15 mol %) which may be assigned to the Ca 3 Ti 2 O 7 phase (JCPDS -78-2480). The amount of volume fraction of crystalline phase X c was calculated by comparison of integral intensities from X-ray diffraction patterns of amorphous and completely crystalline samples as per the method reported by A. G. Ilinsky et al [17]. With increase in X mol%, in the present series the amount of PT crystalline phase is observed to increase.…”

The crystal fraction determination of the nanocrystalline phase transformed from the Fe-base amorphous matrix using EXAFS

“…HREM observation requires a difficult sample preparation and thermal analysis has an ambiguity in the enthalpy determination because of the structural relaxation during heat treatment and the interface effect of nanocrystal. And X-ray experimental methods such as extended X-ray absorption fine structure (EXAFS), anomalous X-ray scattering method, and small angle X-ray scattering have been introduced to examine the nanocrystal structure [6][7][8]. These analysis techniques have an advantage such as non-destructive test, statistical averaging, and easy sample preparation.…”