The Emirates Ultraviolet Spectrometer (EMUS) onboard the Emirates Mars Mission (EMM) Hope probe images Mars at wavelengths extending from approximately 100 to 170 nm. EMUS observations began in February 2021 and cover over a full Mars year. We report the first limb scan observations at Mars of ultraviolet emissions Ar I 106.6 nm, N I 120 nm, and carbon monoxide (CO) Fourth Positive Group (A − X) band system excited by electron impact on CO. We use EMUS limb scan observations to retrieve number density profiles of argon, molecular nitrogen, atomic oxygen, and CO in the upper atmosphere of Mars from 130 to 160 km. CO is a sensitive tracer of the thermal profile and winds in Mars' middle atmosphere and the chemistry that balances CO2 in the atmosphere of Mars. EMUS insertion orbit special observations demonstrate that far ultraviolet limb measurements of the Martian thermosphere can be spectroscopically analyzed with a robust retrieval algorithm to further quantify variations of CO composition in the Martian upper atmosphere.