Environmentally Friendly and Highly Efficient Co(OAc)2-Catalyzed Aerobic Oxidation to Access 2,6-Di-Electron-Donating Group Substituted 4-Hydroxybenzaldehydes
A catalyst-free, direct electrooxidative phenols derivatives C(sp3)−H mono- and di-alkylations have been developed. In contrast to previous typical oxidative and electrochemical coupling, this electrosynthetic approach enabled selective mono- and di-alkylations...
Herein, with the aim of comprehensive utilization of a useless by-product, a highly selective method was proposed for the production of 5-methyl vanillin by employing o-vanillin, a useless by-product in the vanillin industry, as a raw material.
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