“…5,18 In this context, several methods for determining free glycerol in biodiesel have been proposed, aiming at a more viable, simple, and environmentally friendly. [14][15][16][17][18][19][20][21][22][23][24][25][26][27][28][29][30][31] Among these methods, approaches employing electroanalytical, 15,[19][20][21] chromatographic, 14,[22][23][24] electrophoretic, 17,25 spectrophotometric 16,[26][27][28][29][30] or volumetric 31 techniques have been evaluated. However, most of these methods require the use of chemical reagents and organic solvents, such as derivatization reagents, dissolution solvents, and adsorbents, or specic devices (electrodes, apparatus, glassware, cartridges), which are not accessible and very expensive, maintaining necessary the search for a simple method for the determination of free glycerol in biodiesel.…”