Ethylene glycol assisted spray pyrolysis for the synthesis of hollow BaFe12O19 spheres

Abstract

a b s t r a c tHollow spherical BaFe 12 O 19 particles were synthesized by spray pyrolysis from a solution containing ethylene glycol (EG) and precursors at 1000 1C. The effects of EG concentration on particle morphology, crystallinity and magnetic properties were investigated. The hollow spherical particles were found to consist of primary particles, and higher EG concentration led to a bigger primary particle size. EG concentration did not show much effect on the hollow particle size. Better crystallinity and higher magnetic coercivity were obtained with higher EG concentration, which is attributed to further crystallization with the heat produced from EG combustion. Saturation magnetization (emu/g) decreased with increasing EG concentration due to residual carbon from EG incomplete combustion, contributing as a non-magnetic phase to the particles.Published by Elsevier B.V.

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