This paper discusses the mechanical properties and grain refinement of an AA 7075 aluminum alloy twist-extruded at the cold-working temperature, and variations in the properties caused by prior annealing and as a function of the mechanical properties. Post-processing properties at room temperature, namely, the tensile strength, micro-hardness and microstructure were determined. An increase in the micro-hardness and tensile strength after three passes of twist extrusion (TE) was seen when compared with the starting annealed state. When prior annealing was done at 300°C, the increase in the micro-hardness was 37 % and the increase in the tensile strength was 5 %. The corresponding figures for prior annealing at 400°C were 34 % and 4 %, respectively, while for the 500°C prior annealing, the figures were 31 % and 3 %, respectively. However, the rate of increase in the micro-hardness and tensile strength of a sample in the annealed state was higher at 300°C than at 400°C or 500°C. In addition, a very fine structure of the AA 7075 aluminum alloy developed during the three TE passes as observed with a scanning electron microscope.