Extraction and identification by GC-MS of phenolic acids in traditional balsamic vinegar from Modena

Plessi, Maria; Bertelli, Davide; Miglietta, Franco

doi:10.1016/j.jfca.2004.10.008

Cited by 78 publications

(54 citation statements)

References 17 publications

(15 reference statements)

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“…[1][2][3][4] Qualitative approaches comprising mass spectral search, retention index and diversified scan technologies were utilized to identify volatile compounds. [5][6][7][8] The combination of these approaches can provide satisfactory identification results for volatile compounds including some trace-level components.…”

Section: European Journal Of Mass Spectrometrymentioning

confidence: 99%

Application of Gas Chromatography-Quadrupole-Time-of-Flight-Mass Spectrometry for Post-Target Analysis of Volatile Compounds in Fructus Amomi

Kang

Zhang

et al. 2013

Eur J Mass Spectrom (Chichester)

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A post-target analysis method based on gas chromatography coupled to a high-resolution quadrupole time-of-flight mass analyzer is applied for the investigation of volatile compounds in Fructus Amomi. A series of narrow window extracted ion chromatograms at selected characteristic ions were performed. Chromatographic peaks with the same retention time in different extracted ion chromatograms was used to screen out the candidate compound. Identification was achieved by the accurate masses of several characteristic ions and the retention index of the peak. Forty six compounds, including 12 monoterpene compounds, were identified by conventional static headspace gas chromatography mass spectrometry and another six monoterpene compounds were found and identified by the post-target method. Post-target analysis is a useful strategy in qualitative research of natural products.

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Section: European Journal Of Mass Spectrometrymentioning

confidence: 99%

Application of Gas Chromatography-Quadrupole-Time-of-Flight-Mass Spectrometry for Post-Target Analysis of Volatile Compounds in Fructus Amomi

Kang

Zhang

et al. 2013

Eur J Mass Spectrom (Chichester)

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“…TBV is appreciated world wide for its extremely high certified quality. Its physicochemical properties have therefore been studied by several authors with regard to carboxylic acids [1], phenolic acids [2], furanic compounds [3], microbiology [4,5], heavy metals [6], as have the relationships between different parameters [7 -9].…”

Section: Introductionmentioning

confidence: 99%

Solid‐phase extraction method for determination of volatile compounds in traditional balsamic vinegar

Durán‐Guerrero

Chinnici

Natali

et al. 2008

J of Separation Science

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A solid-phase extraction method for the determination of volatile compounds in traditional balsamic vinegar (TBV) has been developed. The optimisation has been carried out using a two-level factorial design expanded further to a central composite design. LiChrolut-EN SPE cartridges were used and the optimised analytical conditions were: 7 g of TBV diluted 1:4, 5 mL of washing water, and elution with 10 mL of dichloromethane. The linear ranges and detection and quantitation limits were adequate for the analysis of the studied compounds in TBV. The accuracy of the method was also studied: recoveries up to 80% and repeatability values lower than 15% were obtained for the majority of the studied compounds. Two TBVs of different age were analysed by the optimised method.

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“…The phenol contents of TBV samples were analysed both with colorimetric method (Verzelloni et al 2007) and by gas chromatography-mass spectrometry (GC-MS) (Plessi et al 2006), but the quantitative characterisation of each individual phenolic acid is still unsatisfactory. Natera et al (2003) grouped and classified vinegars on the basis of phenolic composition, aroma compounds, and organic acids.…”

Section: Phenolic Compoundsmentioning

confidence: 99%

“…This new taste seems to better match consumer preferences and is favoured by professional tasting panels who award sweeter vinegars with higher sensory scores. The relationship between composition, maturing time, and sensorial properties of TBV has recently been investigated by various authors, applying a statistical approach to the data (Chinnici et al 2003;Cocchi et al 2002Cocchi et al , 2006Plessi et al 2006;Sanarico et al 2002;Giordano et al 2003;Masino et al 2008). Unfortunately, different conclusions were reached and the relationship between age, composition, and sensorial properties remains an intriguing unresolved question.…”

Section: Tbv Composition Over the Last Three Decadesmentioning

confidence: 99%

The Balsamic Family

Giudici

Lemmetti

Mazza³

2015

Balsamic Vinegars

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Extraction and identification by GC-MS of phenolic acids in traditional balsamic vinegar from Modena

Cited by 78 publications

References 17 publications

Application of Gas Chromatography-Quadrupole-Time-of-Flight-Mass Spectrometry for Post-Target Analysis of Volatile Compounds in Fructus Amomi

Application of Gas Chromatography-Quadrupole-Time-of-Flight-Mass Spectrometry for Post-Target Analysis of Volatile Compounds in Fructus Amomi

Solid‐phase extraction method for determination of volatile compounds in traditional balsamic vinegar

The Balsamic Family

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