Industrial Scale Natural Products Extraction 2011
DOI: 10.1002/9783527635122.ch6
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Extraction Technology

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Cited by 8 publications
(12 citation statements)
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“…In addition to pure ethanol, which had the highest solubility for rutin, we also investigated the extraction kinetics of 70 vol % ethanol, as the addition of water has been shown to improve the extraction kinetics for rutin from plant material. 16 To determine the extraction kinetics shown in Figure 4, 3 g of dried leaf biomass with a particle size between 1.0 and 1.4 mm, which is typical for industrial-scale extractions from plant biomass, 31 was extracted in 0.2 L of each solvent, respectively. Offline HPLC samples (0.8 mL of each) were taken over 6 h at room temperature in stirred batch extraction mode.…”
Section: Methodsmentioning
confidence: 99%
See 1 more Smart Citation
“…In addition to pure ethanol, which had the highest solubility for rutin, we also investigated the extraction kinetics of 70 vol % ethanol, as the addition of water has been shown to improve the extraction kinetics for rutin from plant material. 16 To determine the extraction kinetics shown in Figure 4, 3 g of dried leaf biomass with a particle size between 1.0 and 1.4 mm, which is typical for industrial-scale extractions from plant biomass, 31 was extracted in 0.2 L of each solvent, respectively. Offline HPLC samples (0.8 mL of each) were taken over 6 h at room temperature in stirred batch extraction mode.…”
Section: Methodsmentioning
confidence: 99%
“…16,27 Additionally, the extraction method, biomass pretreatment, and particle size must be optimized on the basis of the extraction kinetics of small-scale industrial-like extractions and an extraction time must be determined, which maximizes the space–time yield. 31 To foster the sustainability of the extraction process, energy costs, extraction time, and solvent input should be minimized.…”
Section: Introductionmentioning
confidence: 99%
“…The main disadvantage of immersion compared with percolation is the need for mechanical separation of the solids after extraction, either by filtration or by centrifugation. This is the reason that the percolation principle is preferred over immersion technology for most industrial scale oil extraction (Pfennig et al, 2011). However, material must not be presented in the form of meal, as this would make solvent percolation impossible.…”
Section: Introductionmentioning
confidence: 99%
“…The reason for the increase in extraction efficiency with smaller particle sizes is the dependence of diffusion on the mass or size of the particles. A smaller particle size reduces the time required for the diffusion of solvents, thus facilitating the direct extraction of the metabolites in the solvents (Pfenning et al ., ). Coats and Wingard () reported how the size and shape of particles significantly affected the extraction of oils from seeds and Sari and Velioglu (), described how the theanine content determined in tea varied according to the size of the ground tea‐leaf particles.…”
Section: Sample Preparationmentioning
confidence: 99%