Fabrication of 316 Ss–B4c Composite by Powder Metallurgical Route

In the current study, metal matrix composites of iron-based alloy (SS316) are successfully cast by the application of a novel processing route of microwave hybrid heating (MHH). The castings of iron-base alloy (SS316) powder and reinforced with 10 wt.% EWAC1004 (Ni-based) + 3 wt.% WC-12Co are developed in the domestic microwave oven power of 900 W and frequency 2.45 GHz. The mechanical and metallurgical properties of the prepared casts are investigated. The value of the mean particle size of the powder used is found to be 40 μm. Scanning electron microscopy (SEM), optical microscopy (OM), X-Ray diffraction (XRD), and Vickers’s microhardness tester are used for the characterization of so developed composites samples. The microstructure is reported as elongated columnar grains or lathlike structure with uniform melting of the iron-based (SS316) matrix has been achieved. The XRD confirmed the presence of typical carbides and intermetallic. The average micro-hardness of the reinforced composites is reported as 420 ± 90 HV0.3. The achieved microhardness of cast samples is 2 times the commercially received SS316. The micro-hardness obtained on the surface of the carbide phase is 648.16 HV0.3. The porosity of the prepared cast is found to be less than 2% which is approximately 3 times less as compared to commercially received SS316. The relative density of the microwave cast SS316 without reinforcement is found to be maximum with the value of 98%. The value of grain size of the microwave-casted composite samples is reduced to 23 microns (μm)

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Processing and characterization of SS316 based metal matrix composite casting through microwave hybrid heating

Pal

Gupta

Singh

2022

Proceedings of the Institution of Mechanical Engineers, Part C:

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Development of iron-based composite materials through electromagnetic radiations in a domestic microwave oven

Pal

Gupta

Singh

2023

Proceedings of the Institution of Mechanical Engineers, Part C:

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Microwave hybrid heating, a novel technique, is used to develop iron-based alloy (SS316), SS316+10EWAC1004 (nickel-based), and SS316+10EWAC1004+5Cr7C3 composite castings. The domestic microwave having a frequency of 2.45 × 103 MHz and a power of 0.9 kW, is used with a variable exposure time of microwave radiations. The microwave interaction procedure with the metallic powder is discussed to optimize the exposure time and temperature. A microstructure study of developed castings revealed the uniform melting of matrix and EWAC1004 with an identical dispersion of Cr7C3. The X-ray diffraction results revealed various intermetallic (Ni3Fe, Ni2Si, Cr2Ni3, MoNi4, Fe3Si, Fe2Si, CrFeNi) and hard carbides (Fe3C, Cr3C2, Cr23C6) phases. The maximum average micro-hardness is for the SS316+10EWAC1004+5Cr7C3 composite, followed by SS316+10EWAC1004. The established composite casting had a hardness of around 2 times that of the commercial SS316. The maximum density of 97% was found for Iron-based SS316-based. The grain size of microwave-processed SS316, SS316+10EWAC, and SS316+10EWAC +5Cr7C3 specimens is found to be 21 ± 4 µm, 18 ± 3 µm, and 17 ± 2 µm, respectively. It has been observed that reinforced phases hinder grain growth, and hence grain size reduces significantly. In comparison, commercial SS316 had a grain size of 31 ± 6 µm. The ASTM B-276 standard is used to determine pores that are of the order of 1.98%.

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Fabrication of 316 Ss–B4c Composite by Powder Metallurgical Route

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Processing and characterization of SS316 based metal matrix composite casting through microwave hybrid heating

Processing and characterization of SS316 based metal matrix composite casting through microwave hybrid heating

Development of iron-based composite materials through electromagnetic radiations in a domestic microwave oven

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