Abstract:Powder of magnesium diboride was obtained by solid phase reaction of mixture of magnesium (> 99% pure) and amorphous boron (> 99% pure) powders at 650-900 °C temperatures in inert atmosphere. During synthesis process main attention was paid to removing oxide layer of surfaces of powder particles by organic solvents in Glovebox, where concentration of oxygen and water steam is less than 5 ppm. Homogenization and activation of powders were conducted in a planetary nano-mill by WC balls in an inert area. Pressing… Show more
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