“…32–34 Because of their adjustable structure, large surface area, good stability, and porous structure, they have a broad application prospect in the field of sample pretreatment. 35–37 The designability of the aromatic ring skeleton and structure of MONs endow them with abundant π–π bonds, hydrogen bonds, and hydrophobic binding sites, which helps to enhance the interaction force with target objects, and thus makes them have great potential for adsorption of organic pollutants. 38,39 However, when MONs are applied to SPE, only a few MONs can be used as an effective adsorbent for extraction due to their small particle size, low density, and unevenness, which is not conducive to recovery.…”