Facile synthesis of antimony-doped tin oxide nanoparticles by a polymer-pyrolysis method

Li, Yuanqing; Wang, Jianlei; Fu, Shao‐Yun; Mei, Shi-Gang; Zhang, Jianmin; Kang, Youngjong

doi:10.1016/j.materresbull.2010.03.003

Cited by 54 publications

(16 citation statements)

References 35 publications

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“…Lower values of resistivity were reported in literature, for pure SnO 2 (2.71 × 10 −2 cm) and 2% Al-doped SnO 2 (6.7 × 10 −2 cm) and the resistivity increased with Al doping level [38]. High resistivity of pure SnO 2 (∼10 K cm) was obtained by Li [39]. Further, minor values of resistivity (172.37 and 704.25 cm) were detected for the Sb-doped SnO 2 sample [40].…”

Section: Electrical Measurementsmentioning

confidence: 61%

Detailed investigation of submicrometer-sized grains of chemically sprayed (Sn1−xAlx, O2) (0≤x≤0.085) thin films

Benhaliliba

Benouis

Yakuphanoğlu

et al. 2012

Journal of Alloys and Compounds

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Section: Electrical Measurementsmentioning

confidence: 61%

Detailed investigation of submicrometer-sized grains of chemically sprayed (Sn1−xAlx, O2) (0≤x≤0.085) thin films

Benhaliliba

Benouis

Yakuphanoğlu

et al. 2012

Journal of Alloys and Compounds

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“…Posthumus et al [4] studied the effect of addition of Sb-SnO 2 particles with grafted 3-methacryloxypropyltrimethoxysilane (MPS) on the electrical resistivity of acrylate films, and the resistivity could be decreased to about 10 2 -10 3 X cm. The resistivity of the Sb-doped SnO 2 synthesized by a facile polymer-pyrolysis method was decreased by more than three orders compared with the pure SnO 2 [5].…”

Section: Introductionmentioning

confidence: 99%

Synthesis and conductive performance of antimony-doped tin oxide-coated TiO2 by the co-precipitation method

Wang

Jiao

Jiang

et al. 2014

J Mater Sci: Mater Electron

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The synthesis of Sb-SnO 2 /TiO 2 (SST) composites by assembling antimony-doped tin oxide (Sb-SnO 2 ) nanoparticles on the surface of titanium dioxide (TiO 2 ) is systematically investigated. X-ray diffraction data show that the SST composite materials with good crystallinity can be indexed as anatase TiO 2 phase and cassiterite SnO 2 phase. The scanning electron microscopy and transmission electron microscopy indicate that Sb-SnO 2 particles with average diameter of 25 nm have been successfully coated on the surface of TiO 2 . In addition, the Ti-O-Sn band can be detected on the surface of TiO 2 through Fourier translation infrared spectroscopy. The influences of pH, Sn/Ti mole ratio, hydrolysis temperature and calcination temperature on the electrical resistivity of the SST powders are studied. Under the optimum experimental conditions, the electrical resistivity of the composite conductive powders is 2.546 9 10 3 X cm. Therefore, the SST composite conductive powders are useful as conductive fillers for the application in antistatic materials.

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“…However, these approaches suffer from some limitations since they usually require a large quantity of solution and organic materials, long processing time, heat treatment for crystallization, filtration, and dry process. Thus, it is of practical importance to seek for a novel method for preparation of metal oxide nanoparticles [11]. The polymer pyrolysis method has some advantages in preparation of nanoparticles: (a) easy operation, (b) easy scale-up in batch form and (c) production of highly homogeneous nanocrystalline particles with excellent magnetic, electrical and optical properties.…”

Section: Introductionmentioning

confidence: 99%

Acrylic acid in the synthesis of a trimetallic nano oxide as NIR reflectance pigment via polymer pyrolysis method

Sharifzadeh¹,

Manteghi

2015

Proceedings of the 19th International Electronic Conference on Synthetic Organic Chemistry

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Recently, the polymer pyrolysis method by means of acrylic acid and metal salts has been developed for preparation of different metal oxides. The co-polymeric precursor compounds are schematically supposed to have metal ions attached by the ionic bonds to carboxylate ions in a polymeric chain or between the polymeric chains. This uniform distribution of metal ions and Ti(OH)4 in the precursor favors the formation of uniformly distributed solid solution of the metallic oxides in the pyrolysis process. In this work, a trimetallic oxide as a pigment with high near-infrared (NIR) reflectance was synthesized by reaction of titanium butoxide with metal acetate (M = Mn, Ni, Ti) in acrylic acid via polymer pyrolysis method. The pigment properties of the oxide were investigated by X-ray diffraction (XRD) and field scanning electron microscopy (SEM), NIR diffuse reflectance spectroscopy (DRS).

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Facile synthesis of antimony-doped tin oxide nanoparticles by a polymer-pyrolysis method

Cited by 54 publications

References 35 publications

Detailed investigation of submicrometer-sized grains of chemically sprayed (Sn1−xAlx, O2) (0≤x≤0.085) thin films

Detailed investigation of submicrometer-sized grains of chemically sprayed (Sn1−xAlx, O2) (0≤x≤0.085) thin films

Synthesis and conductive performance of antimony-doped tin oxide-coated TiO2 by the co-precipitation method

<strong>Acrylic acid in the synthesis of a trimetallic nano oxide </strong><strong>as NIR reflectance pigment <em>via</em> polymer pyrolysis method</strong>

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