Samples of edaphotopes were taken from a depth of 0–15 cm for analyses in this study. It was found that the water in the areas of the Hnidavske swamp and Teremnivski ponds was the most polluted. The level of Zn (0.01 mg/dm3) exceeded the maximum permissible concentration (MPC) at site 5 (Lypnyany village, outside the city of Lutsk, the content was 0.015 mg/dm3) and Hnidavske marsh (0.019 mg/dm3). At all study sites, Cr (0.001 mg/dm3) ranging from 0.002 to 0.005 mg/dm3, Co (0.005 mg/dm3) from 0.008 to 0.01 mg/dm3, and Ni (0.01 mg/dm3) from 0.02 to 0.036 mg/dm3 were also found to exceed the MPC. However, Cd levels (0.005 mg/dm3) did not exceed the MPC and was within the normal range at all study sites (0.0016–0.003 mg/dm3).