Fast and green synthesis of battery-type nickel-cobalt phosphate (NxCyP) binder-free electrode for supercapattery

Gerard, Ong; Ramesh, S.; Ramesh, K.; Numan, Arshid; Khalid, Mohammad; Ramesh, S.; Tiong, S.K.

doi:10.1016/j.cej.2024.154842

Chemical Engineering Journal

2024

DOI: 10.1016/j.cej.2024.154842

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Fast and green synthesis of battery-type nickel-cobalt phosphate (NxCyP) binder-free electrode for supercapattery

Ong Gerard,

S. Ramesh,

K. Ramesh

et al.

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2024

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Enhanced Specific Capacitance and Cycling Stability of Li₂Cu₂(MoO₄)₃ of NASICON Family of Supercapacitor Applications

Dayanithi,

Murugesan,

Annamalai

et al. 2024

ChemistrySelect

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NASICON electrode materials exhibit a broad spectrum of electrochemical potentials, robust ionic conductivity, and structural and thermal stabilities. Using solid state reaction method, Li2Cu2(MoO4)3 was synthesized, a member of NASICON family of compounds based on molybdenum. Various analytical techniques employed to assess structural and morphological properties of synthesized nanomaterial. X‐ray diffraction (XRD) pattern indicated that generated Li2Cu2(MoO4)3 nanomaterial exhibited orthorhombic crystalline structure, with crystallite size of approximately 48 nm. The nanomaterial morphology was evaluated using field emission scanning electron microscopy (FESEM), showing columnar‐ or fiber‐like morphology composed of some conductivity points. The elemental composition of Li2Cu2(MoO4)3 was analyzed by EDAX analysis, confirming the presence of elements lithium, copper, molybdenum, and oxygen. The optical properties and band gap of Li2Cu2(MoO4)3 were analyzed by ultraviolet visible diffuse reflectance spectroscopy (UVDRS). Elemental composition of surface along with electronic states and oxidation states of component present in the nanomaterial Li2Cu2(MoO4)3 were investigated from X‐ray photoelectron spectroscopy (XPS). Electrochemical evaluation using cyclic voltammetry (CV), galvanostatic charge–discharge (GCD), and electrochemical impedance spectroscopic (EIS) showed a specific capacitance of 250 F g−1 at 3.5 A g−1 with the high retention rate of 95.82% after 3000 cycles, indicating its potential for high performance supercapacitors.

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Enhanced Specific Capacitance and Cycling Stability of Li₂Cu₂(MoO₄)₃ of NASICON Family of Supercapacitor Applications

Dayanithi,

Murugesan,

Annamalai

et al. 2024

ChemistrySelect

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show abstract

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Fast and green synthesis of battery-type nickel-cobalt phosphate (NxCyP) binder-free electrode for supercapattery

Cited by 1 publication

References 117 publications

Enhanced Specific Capacitance and Cycling Stability of Li₂Cu₂(MoO₄)₃ of NASICON Family of Supercapacitor Applications

Enhanced Specific Capacitance and Cycling Stability of Li₂Cu₂(MoO₄)₃ of NASICON Family of Supercapacitor Applications

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Fast and green synthesis of battery-type nickel-cobalt phosphate (NxCyP) binder-free electrode for supercapattery

Cited by 1 publication

References 117 publications

Enhanced Specific Capacitance and Cycling Stability of Li2Cu2(MoO4)3 of NASICON Family of Supercapacitor Applications

Enhanced Specific Capacitance and Cycling Stability of Li2Cu2(MoO4)3 of NASICON Family of Supercapacitor Applications

Contact Info

Product

Resources

About

Enhanced Specific Capacitance and Cycling Stability of Li₂Cu₂(MoO₄)₃ of NASICON Family of Supercapacitor Applications

Enhanced Specific Capacitance and Cycling Stability of Li₂Cu₂(MoO₄)₃ of NASICON Family of Supercapacitor Applications