2019
DOI: 10.1002/jssc.201900050
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Fast determination of 14 mycotoxins in chestnut by dispersive solid‐phase extraction coupled with ultra high performance liquid chromatography‐tandem mass spectrometry

Abstract: ochratoxin A, deoxynivalenol, 3acetyldeoxynivalenol, 15-acetyldeoxynivalenol, and zearalenone in chestnut samples.The method was used to analyze 136 samples obtained from Shandong province in China. The mycotoxins were extracted using a dispersive solid-phase extraction method and cleaned using an improved quick, easy, cheap, effective, rugged, and safe approach. The mycotoxins were then detected using a triple-quadrupole mass spectrometer. The limits of detection and quantification ranged from 0.02 to 1 and 0… Show more

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Cited by 23 publications
(17 citation statements)
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“…Four milliliters (10 μg/mL) AFB1 solution (prepared in methanol-water) was added into the tubes. The mixture was vigorously shaken at 2500 rpm for a series of time (1,2,3,6,9,12,15,20,25,30,35,40, and 60 min). The tubes were centrifuged and the supernatants were measured by HPLC.…”
Section: Dynamics Of Polymersmentioning
confidence: 99%
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“…Four milliliters (10 μg/mL) AFB1 solution (prepared in methanol-water) was added into the tubes. The mixture was vigorously shaken at 2500 rpm for a series of time (1,2,3,6,9,12,15,20,25,30,35,40, and 60 min). The tubes were centrifuged and the supernatants were measured by HPLC.…”
Section: Dynamics Of Polymersmentioning
confidence: 99%
“…As one of the most abundant and powerful natural chemical carcinogen, aflatoxins (AFs) have been found to be carcinogenic, teratogenic, and mutagenic to humans. Serious health problems and economic losses caused by this category have become a global issue . Therefore, it is urgent to develop reliable analytical technique for solving mycotoxin problems in various samples employed.…”
Section: Introductionmentioning
confidence: 99%
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“…LC‐MS/MS has been reported and considered as the universal approach for mycotoxin screening due to their high selectivity for analyzing several analyte in one run [17–22]. Recently, a few multi‐mycotoxin analysis methods have been described in varied food commodities, however the validated methods for baby food analysis are rare as high sensitivity is required to satisfy the strict regulation in such types of matrices [7,23].…”
Section: Introductionmentioning
confidence: 99%
“…PA was previously detected in many agricultural products, including animal feed, corns, wheat, nuts, spices and fruits 3,8–13 . Liang et al .…”
Section: Introductionmentioning
confidence: 99%