The low cycle fatigue properties of a I2Cr-I M e V martensitic stainless steel are investigated at room temperature and correlated with its microstructure. The mechanical test results show that the behavior of this steel depends on the applied strain level. The SEM and TEM studies bring out the role of ferrite islands embedded in a tempered martensite lath matrix. Plastic deformation is essentially accommodated by ferrite: this results in extrusion formation on the surface specimen and a cellular dislocation structure. When the strain level is high, it requires a greater contribution of the tempered martensite, ferrite alone being unable to accomplish all the plastic deformation.
1NTRODUCTION12Cr stainless steels are widely used for machine components, such as turbine blades, subjected to stresses at high temperature [I]. For this reason, high temperature data are available concerning creep fracture [2], low cycle fatigue damage [3], and precipitation [4].The I2Cr-IM-V steel is commonly used in a normalized and tempered condition, involving diffusionless transformation of the austenite to martensite and precipitation reactions during tempering accompanied by recovery processes. The physical metallurgy of this alloy is therefore very complex.The objective of the present paper is to correlate the cyclic behavior with the microstructure in order to gain a better understanding of fatigue micromechanisms in this kind of alloy. Indeed if crack initiation mechanisms are well developed and clearly understood for pure materials, this aspect is less well-known for engineering materials, except austenitic stainless steels. Therefore this remains of prime interest especially for practical cases. In the present investigation, only room temperature behaviour is considered in order to eliminate oxydation and temperature effects.
EXPERIMENTSThe material investigated in this work is a type DIN X20CrMoV12-1 steel. Its chemical composition by weight YO is: 0.21 C, 0.006 S, 0.017 P, 0.24 Si, 0.60 Mn, 0.02 Cu, 11.3 Cr, 0.62 Ni, 0.85 Mo, 0.36 V, 0.03 W remainder Fe. The heat treatment of the as-received material consists of austenizing at 1050°C for 1 h followed by air cooling to room temperature and tempering at 760°C for 2 h, also followed by air cooling.Tensile and low cycle fatigue tests are performed at room temperature on a 100 kN servohydraulic push-pull MTS machine. Cylindrical (10 mm diameter and 10 mm gauge length) and button-headed samples are machined from a 24/34 cm diameter pipe. Before testing, the reduced 435