2001
DOI: 10.1080/20015891109329
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Final Evaluation of US EPA Method 3546: Microwave Extraction, a Microwave-Assisted Process (MAPTM)∗ Method for the Extraction of Contaminants Under Closed-Vessel Conditions

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“…Water samples were filtered using GF/F 47 mm filter paper and sediment samples were dried using a lyophilizer. Estrogenic compounds were extracted from water and sediment samples by Solid Phase Extraction (SPE) using a modified Leuscha et al procedure and EPA Method 3546, respectively [ 36 , 37 ]. Briefly, SPE was carried out for 2 L of water samples, using preconditioned Oasis HLB (SPE) cartridges at a flow rate of 10 mL/min while Microwave Assisted Extraction (MAE) was conducted on 5 g of sediment samples.…”
Section: Methodsmentioning
confidence: 99%
“…Water samples were filtered using GF/F 47 mm filter paper and sediment samples were dried using a lyophilizer. Estrogenic compounds were extracted from water and sediment samples by Solid Phase Extraction (SPE) using a modified Leuscha et al procedure and EPA Method 3546, respectively [ 36 , 37 ]. Briefly, SPE was carried out for 2 L of water samples, using preconditioned Oasis HLB (SPE) cartridges at a flow rate of 10 mL/min while Microwave Assisted Extraction (MAE) was conducted on 5 g of sediment samples.…”
Section: Methodsmentioning
confidence: 99%