We present the first experimental determination of the time auto-correlation of magnetization in the nonstationary regime of a spin glass, and its quantitative comparison with the corresponding response, the magnetic relaxation function. These measurements were performed in a new experimental setup working as an absolute thermometer. Clearly, we observe a non-linear fluctuation-dissipation relation between correlation and relaxation, i.e. an effective temperature higher than the bath temperature in the aging regime. According to theoretical developments on mean field models, and lately on short range ones, in the limit of very large waiting times, the relation between relaxation and correlation in the aging regime becomes temperature independent for a given system. A scaling procedure allows us to extrapolate to the limit of long waiting times by separating stationary and non-stationary regimes and to check the validity of the temperature independence of the fluctuation dissipation relation in the non-stationary regime.