2010
DOI: 10.1002/adsc.201000130
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Fluorous Surface‐Active Distannoxane Catalysts

Abstract: Abstract:Fluorous distannoxanes (XR f 2 SnOSnR f 2 X) 2 ·n H 2 O (R f = C 6 F 13 C 2 H 4 ) (1: X= C 8 F 17 SO 3 , n = 10; 4: X= Cl, n = 0) (1) catalyze the Mukaiyama aldol reaction and the allylation of aldehydes with tetraallyltin at room temperature in fluorous/organic biphasic solvent systems, in which the reactions proceed more rapidly than in a single organic or fluorous solvent. Due to the unique surface activity of 1, the catalyst, organic substrate(s), and reagent(s) are distributed in both organic and… Show more

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“…The use of triorganotin hydrides in organic synthesis is well documented . There have also been several reports on the use of organooxotin compounds as catalysts particularly in esterification reactions …”
Section: Introductionmentioning
confidence: 99%
“…The use of triorganotin hydrides in organic synthesis is well documented . There have also been several reports on the use of organooxotin compounds as catalysts particularly in esterification reactions …”
Section: Introductionmentioning
confidence: 99%