Formation of palladium nanoparticles under pulse current in a dimethylformamide solution

Surface analysis of nickel nanomaterials electrodeposited on graphite surface

“…), geometry and even chemical composition. From the technical point of view, pulse electrolysis in aprotic organic solvents might be very convenient [1][2][3][4][5]. Pulse electrolysis is considered as a sort of non-stationary electrodeposition of metals that influences nucleation process and particle growth.…”

“…Experimental 2.1. Electrochemical deposition of pure Ni and Ni-Pd: Pure Ni was deposited in (CH 3 ) 2 SO (99%, Аlfa Аesar) solution with 0.1 M NiCl 2 (98%, Sigma Aldrich) at 35°С in a three-electrode thermostated glass electrolyser with a volume of 50 cm 3 . The solution of 0.05 M Bu 4 NClO 4 (99.0%, Sigma Aldrich) in DMSO was used as supporting electrolyte for higher electroconductivity.…”

Preparation and Electrochemical Properties of a Gallium-Doped Zinc Oxide Electrode Decorated with Densely Gathered Palladium Nanoparticles

“…18 Electrodeposition is commonly used to rapidly prepare PdNP-ITOs at room temperature without functionalizing the ITO surfaces. 11,19,[22][23][24][25] The control of NP size and the achievement of a homogeneous distribution of metal NPs across the substrate surface pose challenges in electrodeposition. These challenges result from the rapid electron deposition rates applied in this technique.…”