Formation of strontium-doped lanthanum manganite (La0.8Sr0.2MnO3) by mechanical milling without media balls

Room temperature mechanosynthesis of the La1−Sr MnO3± (0≤x≤1) system and microstructural study

“…This LSM system has been synthesized by several techniques [11][12][13][14][15][16][17][18][19][20][21][22][23]; however there are very few works [24][25][26][27][28][29] The aim of this study is to synthesize by a very simple method (one hour using a planetary ball milling equipment at room temperature) eight phases belonging to the system La 1-x Sr x MnO 3±δ (x=0, 0.25, 0.5, 0.75, 0.80, 085, 0.90, and 1) and analyze the structure before and after annealing at 1100º C in static air. The evaluation of how the x value affects the final structure and symmetry, and how far-in terms of the x value-the solid solution is kept were considered.…”

Electrochemical and mechanical properties of solid oxide fuel cell Ni/YSZ anode fabricated from NiO/YSZ composite powder

“…The compact was co-sintered at 1350°C for 2 h in air to fully densify the electrolyte film. After the sintering, cathode layer consisted of La 0.8 Sr 0.2 MnO 3 (LSM) 21) was deposited on the electrolyte surface by screen printing. Finally the cell was sintered at 1100°C for 2 h in air.…”

Smart Powder Processing for Advanced Materials

“…These results indicated that the presented plasma processing was capable of modifying TiO2 nano-powder to improve its photoreactivity without much reduction in specific surface area, which typically occurred when powder modification was carried out with annealing treatment 34) . Using the features of particle bonding technique, new one-pot processing to synthesize nanoparticles without any heat support was developed [28][29][30][31][32][33] . First, a rapid synthesis of perovskite type lanthanum manganite starting from a mixture of industrial grade powders was demonstrated.…”

“…Adding to the synthesis of LaMnO3 δ , strontium doped materials were also synthesized by the one-pot processing 29,30) . Furthermore, BaTiO3 was also rapidly synthesized by the one-pot processing shown in Fig.…”

“…Fur thermore, by making use of these features, a new one-pot processing method to synthesize nanoparticles without applying extra heat was developed. A rapid synthesis of perovskite type lanthanum manganite and related compounds star ting from a mixture of industrial grade powders was demonstrated [28][29][30][31][32][33]. Also, particle bonding with electric discharge is an interesting phenomenon for controlling surface structure of nanoparticles 34).…”