Frequency Response Evaluation as Diagnostic and Optimization Tool for Pulsed Unipolar Plasma Electrolytic Oxidation Process and Resultant Coatings on Zirconium
Evgeny Parfenov,
Ruzil Farrakhov,
Veta Aubakirova
et al.
Abstract:This study aims to bridge various diagnostic tools for the development of smart plasma electrolytic oxidation (PEO) technologies. PEO treatments of commercially pure Zr were carried out using the pulsed unipolar polarisation (PUP) regime with frequency sweep in an alkaline phosphate-silicate electrolyte. Methods of in situ impedance spectroscopy and electrical transient analysis were used for the process diagnostics under the video imaging of the PEO. Two cutoff frequencies, 170–190 Hz and 620–650 Hz, were ide… Show more
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